Specifications


Endstations or Setup

SuperESCA Main

SpectrometerHemispherical Electron Energy Analyzer SPECS Phoibos 150:
- mean radius 150 mm
- energy resolution < 5 meV
- acceptance angle up to ±13°
- home made 1D delay line detector
Base Pressure8 * 10-11 [mbar]
Detectors Available1D Delay Line Detector
Endstation OperativeYes
Sample
Sample TypeCrystal, Amorphous
Other Sample TypeNanostructured samples
Mounting TypeCustom mounting plate or modified CTPO sample holder
Required Sample SizeX = 9 [mm], Y = 9 [mm], Z = 1 [mm]
Techniques usage
Absorption / NEXAFSAbsorption spectra are measured in Auger yield.
By changing sample orientation, the angle between the electric field E of the polarized light and and the normal to the sample surface can be varied in the range from 20 to 90 degrees.
Photoelectron emission / Angular Resolved PESThe technique is available if the modified CTPO manipulator is used, which allows software controlled angular movements of the samples.
Photoelectron emission / Photoelectron diffractionCore level intensity is measured as a function of polar and azimuthal emission angles. The technique is available if the modified CTPO manipulator is used, which allows software controlled angular movements of the samples.
Photoelectron emission / Time-resolved studiesFast XPS allows monitoring the evolution of core level spectra (typical acquisition time between 4 and 10 seconds per spectrum), e.g. while exposing the sample to gases or during an annealing.
Manipulator or Sample stage
Manipulator
Degrees Of Freedom5
Cradles1
Positioning PrecisionX = 20 [um], Y = 20 [um], Z = 500 [um]
Range Of MovementX = 25 [mm], Y = 25 [mm], Z = 500 [mm]

Sample Holders
Custom sample holder
TypeThe custom sample plate is designed for mounting samples on the LHe cyrostat.
DescriptionThe LHe cryostat, combine with radiative or electron bombardment heating, allows stabilizing the sample temperature in the range between 15 K (80 K if liquid nitrogen is used) and 1500 K .
Only polar angle rotations are allowed.
Sample transfer is not possible.

Modified CTPO holder
TypeSample holder for the modified CTPO manipulator devoted to angular resolved measurements.
DescriptionThe sample holder allows radiative sample heating between 300 and 1100 K.
Polar and azimuthal rotations are possible.
The systems allows sample exchange by means of a fast entry lock.


Last Updated on Friday, 08 March 2019 11:20