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XRD1 Specifications
Page 3 of 6
Main Setup
Gonimeter Type |
Huber Kappa Goniometer |
Circle Axis |
Omega - Kappa - Phi - 2Theta (for detector)
Two rotational stages assembled together in a 60° kappa geometry.
A further circle rotates the Kappa unit around a horizontal axis.
|
Linear Axis |
XYZ-stage on top of Phi for the fine adjustment of the sample |
Sphere of Confusion |
20 µm |
Standard Configurations |
Left (Kappa = 0) for data collection
Top (Kappa = -109.471 Omega = -125.264) for sample mounting
Bottom (Kappa = 109.471 Omega = 54.736) for grazing incidence experiments
Triclinic (Kappa=-30 Omega=54.736) for merging with Left to get completeness on triclinic crystal systems |
Alignment Base |
5 axis Optical Table for alignment of the Goniometer with Beam with feedback from 4-quadrants Beam Position Monitor (Alibava) |
Notes |
XYZ-stage with standard mount according to ACA/IUC for Huber/Hampton standard goniometer heads
Motor and signal currents are transmitted via slip rings enabling unrestricted kappa and phi rotation.
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Accessories
Goniometer Heads |
XYZ Standard; XYZ Short Standard; XYRyRx
Magnetic base or Brass specimen pin |
Additional Stage |
XZTheta additional stage (used in general for High Pressure Cell alignment) |
Temperature Control |
Oxford Cryostrem 700: N2 laminar flow for temperature range 80 – 400 K |
Sample Changer |
Internally developed. |
Last Updated on Monday, 29 May 2023 10:40